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Materials and methods The experimental design and timeline are summarized in Fig

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A solution of compound 1-Methoxy-1-(trimethylsilyloxy)-2-methyl-1-propene (870 mg, 5 mmol), trimethylacetyl chloride (660 mg, 5.5 mmol), TiCl 4 (1.13 g, 6 mmol) and dry DCM (20 mL) was stirred at 0 C under an Ar atmosphere